AFM University Introduction to Atomic Force Microscopy by Paul West

« Cover
« Foreward
« Chapter 1
 « Chapter 2
 
2.1. Basic Concepts
2.2. The AFM Stage
2.2.1 XYZ Scanners
2.2.2 Force Sensors
2.2.3 Integrating LL-Force Sensors and Scanners
2.2.4 Z Motors-Probe Approach
2.2.5 X-Y Stage
2.2.6 Optic Microscope
2.2.7 Mechanical Loop
2.3 Electronics
2.4 AFM Acquisition Software
2.5 LL-AFM Cantilevers and Probes
2.6.1 Vibrations
2.6.2. Environmental Scanning
2.6.3 Heating/Cooling Stages
2.6.4 Higher Speed AFM Scanning
 « Chapter 3
 « Chapter 4
 « Chapter 5
 « Chapter 6
 « Chapter 7
« Appendix A
« Appendix B
« Appendix C
« Appendix D
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Such methods are very computer intensive and it can take a long time to analyze a single image. For example, to do the blind reconstruction on a single 256 X 256 pixel image with an 3 GHz Pentium PC can take 10 minutes.
Probe Damage
The quality of an AFM image is critically dependent on the shape of the probe used for measuring an image. The AFM probe can be severely damaged by tip approach (see Section 3.3). Handling the probe incorrectly before it is placed in the microscope can also cause probe damage. For example, if the probe is exposed to high electric fields, the probe tip can be blown off by electrostatic discharge. Finally, the probe tip can get dirty from the packing materials used to hold the probe while shipping.
Multiple Probes
The scan rate of an AFM limits the sizes of areas that can be analyzed to a few hundred microns at best. It would be highly desirable to create an AFM with multiple probes that could scan many areas simultaneously. Several efforts to create “multiple probe” atomic force microscopes demonstrated that it is possible. In the first approach, several AFM scanners were positioned above a silicon wafer and scanned independently. In the second approach, several probes on a silicon wafer were used to scan a sample simultaneously. The greatest challenge for creating multiple probe AFM instrumentation is to get all of the probes to be as sharp as is required for high resolution scanning.
Calibration of Cantilever Force Constants
As illustrated in Figure 2-40, there is considerable variability in the force constant of an AFM cantilever because of variations primarily in the thickness of the cantilevers. Thus, if the exact force is required for an AFM scan or F/D curve, the force constant for the cantilever used for the tests must be calculated. The primary method used for doing this is the Sader Method. In this method, the physical geometry of the cantilever is measured with an optical microscope and the quality factor, Q, is measured. These parameters are then used in an equation that calculates the force constant, (see Figure 2-43).
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